Low Energy Electron Microscopy


| Adaptation of the standard SEM to SLEEM | | Study of surfaces by very slow electrons | | Non-charging electron microscopy | | Development of ultrahigh-vacuum microscope – SLEEM | | The low voltage transmission electron microscope |





The team deals with low and very low energy scanning electron microscopy and its applications. Its activity focuses on the methodology, instrument principles and unique parts of the instrumentation enabling achieving high resolution imaging at electron energies down to units of electronvolts. The main tasks are the elaboration of methods based on variable electron beam energy along the microscope column and the exploration of retarding optical elements. Important problems are the detection of signal electrons emitted at very low energies, resolution of low energy images, specimen preparation techniques and vacuum problems. The main application fields are the study of very clean and defined surfaces including those prepared in-situ in ultrahigh vacuum, observation of real surfaces under medium voltage conditions, observation of non-conductive specimens and comparison of the low energy image signals with electron-spectroscopical signals, e.g. Auger electrons.


Research topics


Adaptation of the standard SEM to SLEEM
A relatively simple mode enabling work at low and very low energies has been developed in a standard scanning electron microscope. The image resolution is achieved even below 10 nm at the energy of primary electrons of 10 eV and less.
Study of surfaces by very slow electrons
We have been dealing with study of surfaces by electron beam in the range of energies from 0 eV to 20 keV with spatial resolution of units of nm. The properties of doped silicon as well as the layer for x-ray mirrors and opto-electronic elements, growth of single-crystal layers etc. have been studied.
Non-charging electron microscopy
Automatic procedure has been developed for finding an optimum energy of the primary electron beam, at which accumulation of the charge in a specimen does not occur and it is possible to image non-conductive specimens in their original stage without coating with conductive layers.
Development of ultrahigh-vacuum microscope – SLEEM
UHV SLEEM consists of an observation and preparation chamber and a vacuum air lock. The working pressure is 10-8 Pa. The observation chamber is equipped with a field emission source of electrons, adaptation to microscopy by very slow electrons, mass spectrometer and manipulator enabling an accurate tilt in two directions. The preparation chamber is equipped with a ion source and a possibility of evaporation.
The low voltage transmission electron microscope
The low voltage transmission electron microscope is intended for the study of objects composed of atoms with low atomic numbers, such as biological specimens. By decreasing the accelerating voltage, the image contrast increases many times but at the same time the attainable resolution limit decreases, owing to the diffraction limit and chromatic aberration of the objective lens. The obtained results are very promising. A number of technical problems were solved due to which the repeated attempts to realise a low voltage microscope failed in the past. The activities are oriented towards correction of optical aberrations (aperture and chromatic ones), alignment automation, astigmatism correction, image computer focusing, and an increase in electron to light image conversion efficiency.

 
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